Stable Prenucleation Calcium Carbonate Clusters Define Liquid–Liquid Phase Separation

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Stable prenucleation calcium carbonate clusters.

Calcium carbonate forms scales, geological deposits, biominerals, and ocean sediments. Huge amounts of carbon dioxide are retained as carbonate ions, and calcium ions represent a major contribution to water hardness. Despite its relevance, little is known about the precipitation mechanism of calcium carbonate, and specified complex crystal structures challenge the classical view on nucleation c...

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Stable prenucleation mineral clusters are liquid-like ionic polymers

Calcium carbonate is an abundant substance that can be created in several mineral forms by the reaction of dissolved carbon dioxide in water with calcium ions. Through biomineralization, organisms can harness and control this process to form various functional materials that can act as anything from shells through to lenses. The early stages of calcium carbonate formation have recently attracte...

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Prenucleation Clusters and Non-classical Nucleation

In this contribution, we review the recent literature on an alternative crystallization pathway involving stable clusters prior to nucleation and show that the prenucleation cluster pathway is a truly non-classical concept of nucleation. Prenucleation clusters are solutes with "molecular" character in aqueous solution. It becomes evident that the stable clusters may have been concealed by the s...

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Phase transitions in biogenic amorphous calcium carbonate.

Crystalline biominerals do not resemble faceted crystals. Current explanations for this property involve formation via amorphous phases. Using X-ray absorption near-edge structure (XANES) spectroscopy and photoelectron emission microscopy (PEEM), here we examine forming spicules in embryos of Strongylocentrotus purpuratus sea urchins, and observe a sequence of three mineral phases: hydrated amo...

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Freeze-drying yields stable and pure amorphous calcium carbonate (ACC).

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ژورنال

عنوان ژورنال: Angewandte Chemie International Edition

سال: 2020

ISSN: 1433-7851,1521-3773

DOI: 10.1002/anie.201915350